Tensile testing in high-pressure gaseous hydrogen using the hollow specimen method

Abstract Metallic materials, predominantly steels, are the most common structural materials in the various components along the hydrogen supply chain. Ensuring their sustainable and safe use in hydrogen technologies is a key factor in the ramp-up of the hydrogen economy. This requires extensive materials qualification, however, most of the accepted; and standardized test methods for determining the influence of gaseous hydrogen on metallic materials describe complex and costly procedures that are only available to a very limited extent worldwide. The hollow specimen technique is a simple, rapid, and economical method designed to overcome the limitations of the current methods for the qualification of metallic materials under high-pressure hydrogen gas. However, this technique is not yet standardized. The TransHyDE-H2Hohlzug project is presented in this article, along with the main steps required to optimize the hollow specimen technique. This includes closing knowledge gaps related to the specimen geometry, surface quality, and gas purity in dedicated working packages, thus contributing to a comprehensive standardization of the technique for tests in high-pressure hydrogen gas. Impact statement The hydrogen economy is considered a key solution for achieving climate neutrality in Europe, as it plays a crucial role in the decarbonization of sectors such as transport, industry, power, etc. Ensuring the safety and reliability of infrastructure is crucial for the ramp-up of the hydrogen economy. Therefore, it is necessary to meticulously study the materials and components used for infrastructure under conditions that closely resemble in-service conditions. The currently standardized methods are limited as they do not precisely replicate in-service conditions, and when they do, they are often complex, costly, and not easily accessible. This article presents the hollow specimen technique, a simple, and economical method developed to address the limitations of current standardized methods. The results from this work will contribute to the standardization of this technique for tests in high-pressure hydrogen gas. This will enable a faster evaluation of materials for hydrogen applications by industry and academia, thereby contributing to the growth of the hydrogen economy. Graphical abstract

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Publication Details

Journal
MRS Bulletin
Published
2024-09-16
DOI
https://doi.org/10.1557/s43577-024-00776-9
Citations
9
Primary Topic
Hydrogen embrittlement and corrosion behaviors in metals
Type
article
Field-Weighted Citation Impact
1.55

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article

Tensile testing in high-pressure gaseous hydrogen using the hollow specimen method

Mohamed Tlili, Denise Beitelschmidt, Florian Konert, Thorsten Michler et al.
9 citations
MRS Bulletin
Hydrogen embrittlement and corrosion behaviors in metals
1.55
article

Tensile testing in high-pressure gaseous hydrogen using the hollow specimen method

Mohamed Tlili, Denise Beitelschmidt, Florian Konert, Thorsten Michler, Tomás Freitas, Oded Sobol, Heiner Oesterlin, Ken Wackermann, Jonathan Nietzke, Thomas Systermans, Zephanja Krzysch, Stephan Elsen-Humberg, Timo Koenigs, Peter Ruchti, Thomas Böllinghaus
article en
9 citations

Abstract

Abstract Metallic materials, predominantly steels, are the most common structural materials in the various components along the hydrogen supply chain. Ensuring their sustainable and safe use in hydrogen technologies is a key factor in the ramp-up of the hydrogen economy. This requires extensive materials qualification, however, most of the accepted; and standardized test methods for determining the influence of gaseous hydrogen on metallic materials describe complex and costly procedures that are only available to a very limited extent worldwide. The hollow specimen technique is a simple, rapid, and economical method designed to overcome the limitations of the current methods for the qualification of metallic materials under high-pressure hydrogen gas. However, this technique is not yet standardized. The TransHyDE-H2Hohlzug project is presented in this article, along with the main steps required to optimize the hollow specimen technique. This includes closing knowledge gaps related to the specimen geometry, surface quality, and gas purity in dedicated working packages, thus contributing to a comprehensive standardization of the technique for tests in high-pressure hydrogen gas. Impact statement The hydrogen economy is considered a key solution for achieving climate neutrality in Europe, as it plays a crucial role in the decarbonization of sectors such as transport, industry, power, etc. Ensuring the safety and reliability of infrastructure is crucial for the ramp-up of the hydrogen economy. Therefore, it is necessary to meticulously study the materials and components used for infrastructure under conditions that closely resemble in-service conditions. The currently standardized methods are limited as they do not precisely replicate in-service conditions, and when they do, they are often complex, costly, and not easily accessible. This article presents the hollow specimen technique, a simple, and economical method developed to address the limitations of current standardized methods. The results from this work will contribute to the standardization of this technique for tests in high-pressure hydrogen gas. This will enable a faster evaluation of materials for hydrogen applications by industry and academia, thereby contributing to the growth of the hydrogen economy. Graphical abstract

MRS BulletinVol. 49(11)
Federal Institute For Materials Research and Testing (DE), Netzsch (Germany) (DE), Fraunhofer Institute for Mechanics of Materials (DE), Deutscher Verein des Gas und Wasserfaches (DE), Westsächsische Hochschule Zwickau (DE), RWE (Germany) (DE)
Bundesministerium für Bildung und Forschung
Openalex Percentile: Top 19%
Hydrogen embrittlement and corrosion behaviors in metals
1.55
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