Unveiling the Influences of In Situ Carbon Content on the Structure and Electrochemical Properties of MoS2/C Composites

In this work, a MoS₂/C heterostructure was designed and prepared through an in situ composite method. The introduction of carbon during the synthesis process altered the morphology and size of MoS₂, resulting in a reduction in the size of the flower-like structures. Further, by varying the carbon content, a series of characterization methods were employed to study the structure and electrochemical lithium storage performance of the composites, revealing the effect of carbon content on the morphology, structure characteristics, and electrochemical performance of MoS₂/C composites. The experimental setup included three sample groups: MCS, MCM, and MCL, with glucose additions of 0.24 g, 0.48 g, and 0.96 g, respectively. With increasing carbon content, the size of MoS₂ initially decreases, then increases. Among these, the MCM sample exhibits the optimal structure, characterized by smaller MoS₂ dimensions with less variation. The electrochemical results showed that MCM exhibited excellent electrochemical lithium storage performance, with reversible specific capacities of 956.8, 767.4, 646.1, and 561.4 mAh/g after 10 cycles at 100, 200, 500, and 1000 mA/g, respectively.