In Vitro Evaluation of Speed Sintering and Glazing Effects on the Flexural Strength and Microstructure of Highly Translucent Multilayered 5 mol% Yttria-Stabilized Zirconia
This study aimed to investigate the impact of speed sintering and glazing on the flexural strength and microstructure of multilayered 5 mol% yttria-stabilized (5Y-) zirconia, which remains unknown. Bar-shaped specimens (N = 600) were fabricated from 5Y-zirconia (FX; Ceramill Zolid FX ML, ST; Katana STML) by cutting, polishing, sintering (conventional and speed sintering), and then glazing. A flexural strength test (n = 30/group), field emission scanning electron microscopy (FE-SEM) observation (n = 2/group), and an X-ray diffraction (XRD) study with Rietveld refinement (n = 1/group) were performed. The flexural strength was analyzed using three-way ANOVA and a post hoc Scheffé test. The grain size was analyzed using the Kruskal-Wallis H test and Bonferroni-Dunn post hoc test. Flexural strength slightly decreased in the nonglazed FX after speed sintering (<i>p</i> < 0.05). Glazing with and without glazing paste did not affect flexural strength at both sintering speeds (<i>p</i> > 0.05). Speed sintering and glazing minimally changed the Weibull modulus and phase fraction, and did not affect grain size (<i>p</i> > 0.05). ST had a larger grain size and lower tetragonal phase content than FX and had a lower flexural strength than FX in most groups (<i>p</i> < 0.05). Overall, the multilayered 5Y-zirconia is considered suitable for dental application using speed sintering and glazing.
Authors
- Ji-In Jeong (ORCID: https://orcid.org/0000-0003-1117-4957)
- Hyo‐Joung Seol (ORCID: https://orcid.org/0000-0002-6177-2616)
- Yong Hoon Kwon (ORCID: https://orcid.org/0000-0001-8097-2114)
Institutions
- Pusan National University (KR)
Publication Details
- Journal
- Materials
- Published
- 2024-09-21
- DOI
- https://doi.org/10.3390/ma17184634
- Citations
- 6
- Primary Topic
- Dental materials and restorations
- Type
- article
- Field-Weighted Citation Impact
- 2.41
Funders
- National Research Foundation
- National Research Foundation of Korea
- Ministry of Science and ICT, South Korea