Integrating experimental and theoretical investigations of porous graphite materials with scanning electron microscope image processing

Accurate determination of fractal dimension (FD) and permeability of porous graphite materials (PGM) is essential for applications like porous aerostatic bearings (PABs). This study addresses the need for improved measurement methods by employing image processing and computer vision (IPCV) techniques to enhance FD and permeability accuracy. We aimed to refine these measurements by analysing the effects of image size and magnification on accuracy. The research developed theoretical models based on fractal theory, Darcy's law, and a modified Hagen-Poiseuille gas equation to evaluate these effects. A dual-path X-ray imaging detection system was used for experimental validation. The gauge pressure was varied across the surface of the PGM and volume flow rate was measured. MATLAB was utilized for IPCV, enabling precise FD determination and underscoring the importance of image parameters. Results showed that FD values stabilize at specific image sizes and magnifications, improving accuracy. Linear relationships between pressure gradient and volume flow rate were observed, with permeability stabilizing at high pressures. Porosity values varied among materials: Toyo Carbon (15 %), SGL Graphite (17 %), Super Carbon Graphite (27 %), and poplar porous (30 %). FD obtained through theoretical and scanning electron microscope (SEM) methods had a maximum error of 0.08. The study also found a positive correlation between relative density and image grayscale at the macroscopic level. The findings emphasize the importance of optimizing image size and clarity for accurate PGM analysis, providing crucial insights for PAB design and other advanced applications. • The accurate determination of pore size, coefficient of permeability and fractal dimension of porous graphite material can be calculated by the proposed modified theoretical model. • The coefficient of permeability was unstable at low pressure and becomes nearly stable at high pressures due to a linear relationship between pressure gradient and volume flow rate for all specimens of graphite. • The porosity values for various materials of graphite cannot be same. Thus, it is needed to characterize these materials for their use in aerostatic bearings. • The relative density of the internal structure of materials decreases with the increase in fractal value for materials. • The characterization of porous graphite material affects the synergistic performance of aerostatic bearing depending on the measurement of relevant parameters.

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Publication Details

Journal
Results in Engineering
Published
2024-09-17
DOI
https://doi.org/10.1016/j.rineng.2024.102893
Citations
9
Primary Topic
Electron and X-Ray Spectroscopy Techniques
Type
article
Field-Weighted Citation Impact
1.61
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article

Integrating experimental and theoretical investigations of porous graphite materials with scanning electron microscope image processing

Mariyam Sattar, Awais Mehmood, Muhammad Punhal Sahto, Asif Raza et al.
9 citations
Results in Engineering
Electron and X-Ray Spectroscopy Techniques
1.61
article

Integrating experimental and theoretical investigations of porous graphite materials with scanning electron microscope image processing

Mariyam Sattar, Awais Mehmood, Muhammad Punhal Sahto, Asif Raza, Mujib Ur Rahman, Muhammad Fawad Jamil, Mumtaz A. Qaisrani, Wei Wang
article en
9 citations

Abstract

Accurate determination of fractal dimension (FD) and permeability of porous graphite materials (PGM) is essential for applications like porous aerostatic bearings (PABs). This study addresses the need for improved measurement methods by employing image processing and computer vision (IPCV) techniques to enhance FD and permeability accuracy. We aimed to refine these measurements by analysing the effects of image size and magnification on accuracy. The research developed theoretical models based on fractal theory, Darcy's law, and a modified Hagen-Poiseuille gas equation to evaluate these effects. A dual-path X-ray imaging detection system was used for experimental validation. The gauge pressure was varied across the surface of the PGM and volume flow rate was measured. MATLAB was utilized for IPCV, enabling precise FD determination and underscoring the importance of image parameters. Results showed that FD values stabilize at specific image sizes and magnifications, improving accuracy. Linear relationships between pressure gradient and volume flow rate were observed, with permeability stabilizing at high pressures. Porosity values varied among materials: Toyo Carbon (15 %), SGL Graphite (17 %), Super Carbon Graphite (27 %), and poplar porous (30 %). FD obtained through theoretical and scanning electron microscope (SEM) methods had a maximum error of 0.08. The study also found a positive correlation between relative density and image grayscale at the macroscopic level. The findings emphasize the importance of optimizing image size and clarity for accurate PGM analysis, providing crucial insights for PAB design and other advanced applications. • The accurate determination of pore size, coefficient of permeability and fractal dimension of porous graphite material can be calculated by the proposed modified theoretical model. • The coefficient of permeability was unstable at low pressure and becomes nearly stable at high pressures due to a linear relationship between pressure gradient and volume flow rate for all specimens of graphite. • The porosity values for various materials of graphite cannot be same. Thus, it is needed to characterize these materials for their use in aerostatic bearings. • The relative density of the internal structure of materials decreases with the increase in fractal value for materials. • The characterization of porous graphite material affects the synergistic performance of aerostatic bearing depending on the measurement of relevant parameters.

Results in EngineeringVol. 24
University College Dublin (IE), University of Engineering and Technology Lahore (PK), University of Electronic Science and Technology of China (CN), Institute of Space Technology (PK), Muhammad Nawaz Sharif University of Engineering & Technology (PK), Yangzhou University (CN), Xi'an Jiaotong University (CN), Tsinghua University (CN)
Openalex Percentile: Top 18%
Electron and X-Ray Spectroscopy Techniques
1.61
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