Extraction of anthocyanins from purple sweet potato using supercritical carbon dioxide and conventional approaches
• Ethanol-water-modified supercritical carbon dioxide (SC CO 2 ) was used for extraction. • The extraction of phenolic compounds from purple sweet potatoes (PSP) was optimized. • Modified SC CO 2 provided phenolic yields similar to those of methanolic extraction. • The dominant anthocyanins extracted by both methods were peonidin derivatives. • The SC CO 2 extracts from PSP can be used as coloring agents in the food industry. This research investigates the potential of supercritical carbon dioxide (SC CO 2 ) technology as a green and sustainable approach to improve anthocyanin extraction from purple sweet potatoes (PSP). The study explored different extraction parameters (i.e., temperatures of 35–55 °C, cosolvent concentrations of 10–30 % (w/w), ethanol ratios of 30–70 % (v/v), pressures of 30–40 MPa, extraction times of 120–180 min, and solvent: sample ratios of 25:1–45:1(v/w)), to optimize the total phenolic content (TPC), anthocyanin content (ANC), and antioxidant activity (AA). Additionally, conventional extraction methods using different solvent (ethanol and methanol) mixtures, solvent: sample ratios (15:1; 45:1; 6:1 (v/w)), temperatures (35–50 °C), and extraction times (50–60 min) were performed for the extraction of phenolic compounds from PSP. The highest TPC (340 mg GAE/g dry PSP), ANC (136 mg C3G/100 g dry PSP), and AA (ABTS (7.3 mg TEV/g dry PSP), DPPH (18.2 mg TEV/g dry PSP), and FRAP (1399 mg GAE/100 g)) were achieved with 30 MPa, 35 °C and 20 % cosolvent concentration operated for 180 min. These findings underscore the use of SC CO 2 extraction to obtain anthocyanin extracts that can potentially be used as a coloring agent in the food industry. The proposed SC CO 2 extraction method provides an eco-friendly alternative to conventional methods for extracting phenolic compounds.
Authors
- G. Barros (ORCID: https://orcid.org/0000-0001-5411-3906)
- Arda Tuhanioglu
- Sumanjot Kaur (ORCID: https://orcid.org/0000-0002-6390-0124)
- Leonardo Nora (ORCID: https://orcid.org/0000-0002-4675-1403)
- Ali Ubeyitogullari (ORCID: https://orcid.org/0000-0003-1636-9681)
Publication Details
- Journal
- Applied Food Research
- Published
- 2024-09-13
- DOI
- https://doi.org/10.1016/j.afres.2024.100505
- Citations
- 5
- Primary Topic
- Phase Equilibria and Thermodynamics
- Type
- article
- Field-Weighted Citation Impact
- 0.92
Funders
- National Institute of Food and Agriculture