Investigation of mechanical and wettability properties of commercial pure titanium by surface mechanical attrition treatment

The examination of mechanical and wettability properties of commercial pure titanium (CP-Ti) introduced a novel challenge. The microstructure of samples was analyzed by using OM and SEM micro-images. In this study, the hardness of the surface and cross section of samples was evaluated, and the effect of several surface mechanical attrition treatments (SMATed) on samples was examined. Also, the tensile test was done to compare the effect of SMAT duration on mechanical properties of samples. The contact angle method was then employed to investigate the impact of SAMT duration on the wettability trend. According to results, as the treatment time increases, twins become evident in the deeper layers of the samples. In contrast, the near-surface twins are shorter than those found in the deeper material, signifying the presence of finer grains. Moreover, the elevated hardness in SMATed samples can be attributed to several key factors, including cold work, a rise in defects and twins, and grain refinement. The surface hardness increases across the sample series (up to Ti6) due to the substantial energy input. Nevertheless, it is anticipated that further continuation of the process will result in a constant surface hardness. The increased strength observed in SMATed samples can be attributed to factors such as reduction in grain size and the formation of twins. The wettability results show that the treated surfaces exhibited a significant change in wettability compared to the untreated samples, with a 25% reduction in the contact angle. This is attributed to the surface modifications induced by the treatment process, which introduced more hydrophilic functional groups. The results also show that after 4 h of treatment, the contact angle increases, suggesting that the trend may plateau with additional treatment time.