Fabrication of Platinum-Decorated NiCo-Layered Double Hydroxide Nanoflowers for Electrocatalytic Ammonia Oxidation Reaction

The complete anodic oxidation of ammonia is an important part of direct ammonia fuel cells. Fabricating a high-performance electrocatalyst for ammonia oxidation reaction is meaningful for developing a direct ammonia fuel cell. Herein, we designed one platinum-decorated NiCo-layered double hydroxide nanoflower on Ni foam (Pt-NiCo-LDH-Ni foam) and measured the electrocatalytic performance via the cyclic voltammetry (CV) technique. The experimental results demonstrated that the optimized Pt-NiCo-LDH-Ni foam showed great electrocatalytic performance, with a low overpotential with a value of −0.573 V, a high current density of 17.75 mA cm−2 for the ammonia oxidation reaction, and good stability.