Towards time-reduced cure cycles of epoxy resins for mass production of composites maintaining the thermo-mechanical properties

Abstract Because long curing times hinder the mass manufacturing of composite products, there is a constant quest to develop shorter curing cycles that maintain material quality. The authors recently developed a curing prediction methodology for thermoset composites based on an isoconversional model, which is used in this work to shorten the curing time of real practice processes. The investigation presents two optimized cure cycles devised to reduce the curing times recommended by the resin manufacturer while assure a complete degree of cure and restricting the exothermal flow to avoid undesired overheating. The mechanical (compression, in-plane, and interlaminar shear) and physical ( $$T_\mathrm{{g}}$$ <mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML"> <mml:msub> <mml:mi>T</mml:mi> <mml:mi>g</mml:mi> </mml:msub> </mml:math> , void content, and outgassing) properties of specimens extracted from panels manufactured according to recommended curing cycles and the two time-reduced cycles (up to 72% shorter) presented here, exhibited deviations of less than 4%, and always fell within the acceptable range for the most demanding of industrial sectors: aeronautics. The results support the prediction model’s feasibility to achieve more efficient and productive processes.

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Institutions

Publication Details

Journal
Journal of Thermal Analysis and Calorimetry
Published
2024-08-13
DOI
https://doi.org/10.1007/s10973-024-13442-8
Citations
4
Primary Topic
Epoxy Resin Curing Processes
Type
article
Field-Weighted Citation Impact
0.85

Funders

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article

Towards time-reduced cure cycles of epoxy resins for mass production of composites maintaining the thermo-mechanical properties

Jordi Farjas, N. Blanco, Marc Gascons, J. Costa et al.
4 citations
Journal of Thermal Analysis and Calorimetry
Epoxy Resin Curing Processes
0.85
article

Towards time-reduced cure cycles of epoxy resins for mass production of composites maintaining the thermo-mechanical properties

Jordi Farjas, N. Blanco, Marc Gascons, J. Costa, Daniel Sánchez‐Rodríguez, J. A. González
article en
4 citations

Abstract

Abstract Because long curing times hinder the mass manufacturing of composite products, there is a constant quest to develop shorter curing cycles that maintain material quality. The authors recently developed a curing prediction methodology for thermoset composites based on an isoconversional model, which is used in this work to shorten the curing time of real practice processes. The investigation presents two optimized cure cycles devised to reduce the curing times recommended by the resin manufacturer while assure a complete degree of cure and restricting the exothermal flow to avoid undesired overheating. The mechanical (compression, in-plane, and interlaminar shear) and physical ( $$T_\mathrm{{g}}$$ <mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML"> <mml:msub> <mml:mi>T</mml:mi> <mml:mi>g</mml:mi> </mml:msub> </mml:math> , void content, and outgassing) properties of specimens extracted from panels manufactured according to recommended curing cycles and the two time-reduced cycles (up to 72% shorter) presented here, exhibited deviations of less than 4%, and always fell within the acceptable range for the most demanding of industrial sectors: aeronautics. The results support the prediction model’s feasibility to achieve more efficient and productive processes.

Journal of Thermal Analysis and CalorimetryVol. 150(2)
Universitat de Girona (ES)
Universitat de Girona, Ministerio de Ciencia, Innovación y Universidades, Generalitat de Catalunya, Departament d'Innovació, Universitats i Empresa, Generalitat de Catalunya, Agencia Estatal de Investigación
Industry, innovation and infrastructure
Openalex Percentile: Top 31%
Epoxy Resin Curing Processes
0.85
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